By A. Hassner and C. Stumer (Eds.)
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Additional info for Organic Syntheses Based on Name Reactions
M. Angew. Int. S. Am. SOC. 1958 80 6 Oddo, B. Tfal. 36 g, 1 mmol). 25 g of 2 (87%), bp 112'Cc/ 15 torr.
A. Int. 3 To a solution of KOH (120 g, 2 mol) in water are added o-methoxybenzaldehyde 1 (136 g, 1 mmol) under efficient stirring and external cooling with water. Stirring was maintained until a stable emulsion was obtained. After 24 h at 3OoC the mixture was diluted with water and extracted with Et20. Evaporation of the solvent and vacuum distillation of the residue afforded 55 g of 3 (79%), bp 245-255OC. Acidification of the aqueous solution, extraction with EtnO and evaporation of the solvent gave 2, mp 98-99OC.
1940 704 2 Cologne, J. Bull. Fr. 1955 1312 3 Kimel, W. J. Chem. 1957 22 1611 4 Kimel, W. J. Chem. 1958 23 153 5 Stephen,W. J. Chem. F. J. Heterocycl. Chem.. 1986 23 581 7 Enders, Angew. Ed. L. Tetrahedron Lett. 1995 36 3597 D. 3 g) was heated to 22OoC for 3 h and maintained at this temperature for another 3 h. 25 mol) was collected. 5-89'C. xy)aluminiumhydride (SMEAH) (see 1st edition). & H. Me' WjH NaAIH2(OCH2CH20CH3), in PhH Et20,heat,20h 2 (83 Yo) 1 1 Chan, Ka-Kong J. Org. Chem. 1976 41 62 2 Chan, Ka-Kong J.
Organic Syntheses Based on Name Reactions by A. Hassner and C. Stumer (Eds.)